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Hence, the Ti decreases significantly in the entire process of heating since the nitrogen oxide and vapor are easily released accompanying the thermal decomposition of nitrogen-made up of compounds at very low temperatures [21], that is confirmed because of the TG-IR results. Moreover, it truly is worth noting that FR-PA66 exhibits two decomposition peaks in contrast with pure PA66, plus the Tmax2 is increased than the Tmax1 of pure PA66 irrespective of the information of HCNP. This phenomenon could be due to the dehydration reaction of CNHO groups plus the dehydrogenation response of α-CH2 facilitated because of the R-P· cost-free radical substances developed from HCNP, accelerating the formation on the protective compact char levels [22].
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The microtopography of HCNP is shown in Figure two. The SEM and TEM outcomes Plainly confirmed which the HCNP offers a spherical composition, as well as the diameter with the HCNP microsphere is about 2 um having a sleek surface area.
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The microstructure research on the HCNP and char layers formed through the combustion from the cone calorimetry exam was conducted using the scanning electron microscope ZEISS Sigma HDTM. Photographs were being acquired underneath vacuum in a voltage of 5 kV.
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Regarding the TGA results of FR-PA66, the Tmax1 step by step shifted to the reduced temperature than that on the neat PA66 with raising HCNP as a result of minimal Ti of pure HCNP. Figure 1c demonstrates the Ti of HCNP is 352 °C due to tga66 P-N bond priority breakage concerning HCCP and DABA under reduced temperatures. It truly is attention-grabbing to determine the P-that contains alkanes of FR-PA66 are detected from the TG-IR take a look at under four hundred °C, which is appreciably distinctive within the thermal decomposition goods of pure PA66 [20]. Moreover, the R-P· radicals made by HCNP can catalyze and accelerate the breaking of C-N bonds within the α place on the PA66 molecular chain, leading to the development of unstable amino radicals and carbonyl radicals, resulting in the decomposition with the FR-PA66.